HRID1896045

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID79205

2-Bromo-6-methylpyridine

C6H6BrN

结构：C#CC(C)(O)C1CCN(c2nc(C)ccc2[N+](=O)[O-])CC1

HCID86627357

未命名化合物

PRODUCTS

生成物

结构：Cc1cccc(C#CC(C)(O)C2CCN(c3nc(C)ccc3[N+](=O)[O-])CC2)n1

HCID25181781

未命名化合物

收率 41%

PROCEDURE

实验过程

According to the Method B detailed for Examples 218-226 starting from Compound 312c and using 2-bromo-6-methylpyridine the title compound was prepared. After the work-up, the residue was purified by automated flash liquid chromatography (Horizon™-Biotage) eluting with PE-EtOAc 1:1 affording the title product as a yellow oil. Yield: 41%.