HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1896149Generated: October 31, 2026
Triethyl phosphite → HCID 12182784, compound
https://huagongshe.com/reaction/1896149
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | methyl (2R)-2-(((tert-butoxy)carbonyl)amino)-3-iodopropanoate | HCID 10903591 | — |
| Product | HCID 12182784 | HCID 12182784 | — |
Reaction Steps
Boc-3-iodo-L-Ala-OMe (9.4 g) was dissolved in triethyl phosphite (100 mL). The mixture was heated at 130° C. overnight and evaporated to dryness to give a yellow oil (8.37 g). The compound was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08518912B2 |
|---|
| Source dataset | uspto-grants-2013_08 |
|---|
| ORD ID | ord-9019f6aefd0b4b8baad6123f8fda75e2 |
|---|
| Source note | uspto-grants-2013_08 |
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