HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 57431706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57431706 | HCID 57431706 | — |
Reaction Steps
To a solution of 1-benzyl-piperazine (1.97 ml) and NEt3 (1.9 ml) in DCM (100 ml) was added n-butyl chloroformate (1.47 ml). The mixture was stirred at RT for 2 h. Water was added, the org. phase separated, dried (Na2SO4) and evaporated off to give a yellow oil (3.13 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08518912B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-2e1bee124d2d460eac411c66eee522cc |
| Source note | uspto-grants-2013_08 |