HCID 86672491, compound → HCID 86672492, compound

Participants

Reaction Steps

Compound 208 (64%) was synthesized from compound 205 following the same procedure as for compound 207. 1H NMR (CD3OD, 400 MHz) δ 8.12 (s, 1H), 8.03 (s, 1H), 7.38 (s, 1H), 7.32-7.21 (m, 4H), 7.06-7.02 (m, 1H), 6.90-6.86 (m, 1H), 5.08 (d, J=7.2 Hz, 1H), 4.80 (s, 1H), 4.70 (br s, 2H), 4.01 (d, J=6.4 Hz, 1H), 2.87 (s, 3H), 2.80 (t, J=7.2 Hz, 2H), 2.44 (t, J=6.8 Hz, 2H), 2.02-2.09 (m, 1H), 1.83-1.78 (m, 2H), 1.68-1.54 (m, 5H), 0.89-0.93 (m, 1H). HRMS calculated for C40H37ClFN8O (M+H)+: 699.2763. Found 699.2745.

Provenance & Evidence