Toluene → Oxirane, 2-[(octadecyloxy)methyl]-

Participants

Reaction Steps

In a 2 L-volume four-necked flask equipped with a stirrer, a cooling tube, a thermometer and a dropping funnel, 140 g of the obtained maleic anhydride-modified chlorinated propylene-based random copolymer, 60 g of the ester group-containing acrylic acid copolymer obtained in Production Example 1, 8 g of the stabilizer (stearylglycidyl ether) and 36 g of toluene were added and kneaded at 120° C. for 30 minutes. Subsequently, 8 g of 2-amino-2-methyl-1-propanol was added over 5 minutes, then it was kept for 5 minutes. After that, 970 g of hot water at 90° C. was added over 40 minutes. A reduced pressure treatment was performed to remove toluene. Then the reactant was cooled to room temperature with stirring, yielding an aqueous resin composition of the maleic anhydride-modified chlorinated propylene-based random copolymer.

Provenance & Evidence