HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → 5-Chloro-3-nitro-2-phenoxy-pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromo-5-chloro-3-nitropyridine | HCID 280681 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 5-Chloro-3-nitro-2-phenoxy-pyridine | HCID 57942486 | — |
Reaction Steps
This compound was prepared according to the general procedure A described above using 2-bromo-5-chloro-3-nitro-pyridine (500 mg, 2.11 mmol), phenol (258 mg, 2.75 mmol), K2CO3 (437 mg, 3.16 mmol) and DMF (2 mL). MS m/z: 250.4 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08519135B2 |
| Source dataset | uspto-grants-2013_08 |
| ORD ID | ord-f5e28ee4d09b4bda9820b7145c290a44 |
| Source note | uspto-grants-2013_08 |