Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1898250Generated: November 2, 2026

Chloromethyl Methyl Ether → HCID 58268204, compound

https://huagongshe.com/reaction/1898250

Reaction equation

Participants

RoleNameHCIDCharge
ReactantChloromethyl Methyl EtherHCID 7864—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 58268301HCID 58268301—
SolventTetrahydrofuranHCID 8028—
ProductHCID 58268204HCID 58268204—

Reaction Steps

Prepared from 480 mg (1.10 mmol) of N-(2-bromo-5-chloro-pyridin-3-yl)-3-tert-butyl-4-chloro-benzenesulfonamide, 400 mg of potassium carbonate and 170 μL (1.57 mmol) of methoxymethyl chloride in 2 mL THF using procedure x. Yield: 160 mg of a white solid. LC-MSD, m/z for C17H19BrCl2N2O3S [M+H]+=480.9, 482.9, 484.9

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08519135B2
Source datasetuspto-grants-2013_08
ORD IDord-cc311fef2cd34459bef4bae6293983b5
Source noteuspto-grants-2013_08