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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1898413Generated: October 29, 2026

Oxalic Acid → HCID 178422762, compound

https://huagongshe.com/reaction/1898413

Reaction equation

Participants

RoleNameHCIDCharge
ReactantOxalic AcidHCID 971—
ReactantHCID 178422755HCID 178422755—
SolventAcetoneHCID 180—
ProductHCID 178422762HCID 178422762—

Reaction Steps

To a solution of 2-[(2-chloro-6-fluorophenyl)amino]-7,7-dimethyl-N-[4-(trifluoromethyl)phenyl]-7,8-dihydro-1H-furo[3,2-e]benzimidazole-5-carboxamide (Example-107, 0.100 g) in acetone was added oxalic acid. The reaction mass was refluxed for 3 h. The reaction mass was filtered. The obtained residue was washed with pentane and DEE to afford 0.100 g of the desired product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08519149B2
Source datasetuspto-grants-2013_08
ORD IDord-c21b5aa6ea6643e980541b093150aa22
Source noteuspto-grants-2013_08