HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53977094, compound → HCID 23372384, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53977094 | HCID 53977094 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 23372384 | HCID 23372384 | — |
Reaction Steps
A mixture of methyl 2-formyl-4-methoxycinnamate (15.9 g) and 10% palladium on carbon (2.0 g) in ethyl acetate (200 ml) is shaken under a hydrogen pressure of 45 psi for about 18 hours. The mixture is filtered, concentrated in vacuo, and the residue purified by HPLC, eluting with hexanes/ethyl acetate (3:2), to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05571506 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-4a361d29196048238667824f869c6ddf |
| Source note | uspto-grants-1996_11 |