Methyl iodide → HCID 19612631, compound
Reaction equation
[CH3:1][I:2].[C:3]1([CH2:9][CH2:10][CH2:11][S:12][C:13]2[C:17]([C:18]3[CH:19]=[N:20][CH:21]=[CH:22][CH:23]=3)=[N:16][O:15][N:14]=2)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1>CC(C)=O>[I-:2].[C:3]1([CH2:9][CH2:10][CH2:11][S:12][C:13]2[C:17]([C:18]3[CH:19]=[N+:20]([CH3:1])[CH:21]=[CH:22][CH:23]=3)=[N:16][O:15][N:14]=2)[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Methyl iodide (1 ml, 15 mmol) was added to a solution of 3-(3-(3-phenylpropylthio)-1,2,5-oxadiazol-4-yl)pyridine (7 mmol) in acetone and the reaction mixture was stirred at room temperature for 20 h. and evaporated.
Workup
- customevaporated
Sources & evidence
- ORD record
- ord-4e0014c009a944f3b007209732e0e26c
- Source dataset
- uspto-grants-1996_11
- Patent number
- US05571826
Reaction notes
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