HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1899009Generated: October 30, 2026
Potassium Fluoride → HCID 23373134, compound
https://huagongshe.com/reaction/1899009
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Fluoride | HCID 522689 | — |
| Reactant | 2-Bromo-5-methylbenzene-1-sulfonyl chloride | HCID 15155338 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 23373134 | HCID 23373134 | — |
Reaction Steps
32 g of 2-bromo-5-methylbenzenesulfonyl chloride are dissolved in 75 ml of dioxane, and a solution of 20.6 g of KF in 20 ml of water is added. The mixture is stirred at 45° C. for 48 h, poured into 500 ml of water and stirred subsequently for 30 min, and finally the product is filtered off with suction. 24 g of a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05571842 |
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| Source dataset | uspto-grants-1996_11 |
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| ORD ID | ord-e7dc396e0ef748038edb75cc5152a747 |
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| Source note | uspto-grants-1996_11 |
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