HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 23373258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Cyclohexanone | HCID 7967 | — |
| Product | HCID 23373258 | HCID 23373258 | — |
Reaction Steps
The compound 2,7-di(1-cyclohex-1-enyl)fluorene can be prepared by first forming a Grignard reagent from 2,7-diiodofluorene and magnesium and bromoethane in THF by heating for several days in a Schlenk tube at about 60°-90° C. Then cyclohexanone is added. After acidic workup in hot toluene, the 2,7-dicyclohexenyl fluorene is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05571880 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-118bf6ac8e524f66990e64955d4cb10a |
| Source note | uspto-grants-1996_11 |