HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 22616246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | 4-Iodo-5-methyl-1,2-oxazol-3-amine | HCID 18617350 | — |
| Product | HCID 22616246 | HCID 22616246 | — |
Reaction Steps
N-(4-Iodo-5-methyl-3-isoxazolyl)benzenesulfonamide was prepared from 3-amino-4-iodo-5-methylisoxazole and benzenesulfonyl chloride according to the procedures described in Example 41b. The crude product was purified by recrystallization from ethyl acetate/hexanes to give a brown powder m.p. 138°-141° C., yield 46%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05571821 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-4c4d5950b0bf474c9f0a9fda27c7fd0b |
| Source note | uspto-grants-1996_11 |