反应详情

5-Benzyl-N-(4-Bromo-3-methyl-5-isoxazolyl)thiophene-2-sulfonamide was prepared in the same manner as described in Example 2 from 5-amino-4-bromo-3-methylisoxazole and 5-benzyl-2-thiophenesulfonyl chloride in 22% yield. The product was purified by HPLC (5% CH3CN to 100% CH3CN over 30 min.) to give a solid, m.p. 49°-50° C.

1. customThe product was purified by HPLC (5% CH3CN to 100% CH3CN over 30 min.)
2. customto give a solid, m.p. 49°-50° C.