HCID 22062075, compound → HCID 22998374, compound

HRID 1899731Notes

Reaction equation

HRID 1899731 reaction equation
[S:1]1[CH:5]=[CH:4][C:3](OB(O)O)=[CH:2]1.Br[C:11]1[S:15][C:14]([S:16]([N:19]2[CH:23]=[CH:22][CH:21]=[CH:20]2)(=[O:18])=[O:17])=[CH:13][CH:12]=1>>[S:1]1[CH:5]=[CH:4][C:3]([C:11]2[S:15][C:14]([S:16]([N:19]3[CH:23]=[CH:22][CH:21]=[CH:20]3)(=[O:17])=[O:18])=[CH:13][CH:12]=2)=[CH:2]1

Participants

3

Reactant 2

HCID 22062075HCID 22062075, compoundHCID 23445587N-(5-bromothiophenesulfonyl)pyrrole

Product 1

HCID 22998374HCID 22998374, compound

Procedure

N-[5-(3-thienyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 32C from 3-thienylboric acid and N-(5-bromothiophene-2-sulfonyl)pyrrole in quantative yield. This was purified by recrystallization using hexane/ethyl acetate as solvent.

Workup

  1. customThis was purified by recrystallization

Sources & evidence

ORD record
ord-c22ed42f3dec44f6a02a239f2dea6b27
Source dataset
uspto-grants-1996_11
Patent number
US05571821

Reaction notes

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