HRID1899782
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
200 g (0.97 mol) of methyl (E)-β-methoxy-2-methylcinnamate and 190 g (1.07 mol) of N-bromosuccinimide which has been washed with methanol and dried, in 2 1 of dry tetrachloromethane, are irradiated with a 300 watt UV lamp for 75 min, during which the solution begins to reflux.
WORKUP
后处理
- dry with materialdried, in 2 1 of dry tetrachloromethane
- customare irradiated with a 300 watt UV lamp for 75 min, during which the solution
- temperatureto reflux