1,6-Dichlorohexane → HCID 13360891, compound

HRID 1900546Notes

Reaction equation

HRID 1900546 reaction equation
[C:1]1([CH:7]=[CH:8][N:9]2[C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=3[NH:11][C:10]2=[O:18])C=C[CH:4]=[CH:3][CH:2]=1.[Cl:19]CCCCCCCl>>[Cl:19][CH2:4][CH2:3][CH2:2][CH2:1][CH2:7][CH2:8][N:9]1[C:13]2[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=2[NH:11][C:10]1=[O:18]

Participants

3

Reactant 2

HCID 165511,6-DichlorohexaneHCID 70284256HCID 70284256, compound

Product 1

HCID 13360891HCID 13360891, compound

Procedure

The above mentioned compound was prepared analogously to the procedure described in J. Het. Chem. 18, 85 (1981) from 1-( -phenylvinyl)-2,3-dihydro-1H-benzimidazol-2-one and 1,6-dichloro hexane. The protecting group was then removed by acid hydrolysis with hydrochloric acid following the above procedure. M.p. 80°-84° C.

Workup

  1. customwas prepared analogously to the procedure
  2. customThe protecting group was then removed by acid hydrolysis with hydrochloric acid following the above procedure

Sources & evidence

ORD record
ord-b073ba2394f54a508ee376e73195c117
Source dataset
uspto-grants-1996_11
Patent number
US05576318

Reaction notes

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