2,4-Dichloronitrobenzene → HCID 23369409, compound

HRID 1900548Notes

Reaction equation

HRID 1900548 reaction equation
Cl[C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[N+:9]([O-:11])=[O:10].[CH3:12][O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[N:20]1[CH2:25][CH2:24][N:23]([CH2:26][CH2:27][CH2:28][CH2:29][NH2:30])[CH2:22][CH2:21]1>>[CH3:12][O:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=1[N:20]1[CH2:21][CH2:22][N:23]([CH2:26][CH2:27][CH2:28][CH2:29][NH:30][C:2]2[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=2[N+:9]([O-:11])=[O:10])[CH2:24][CH2:25]1

Participants

3

Reactant 2

HCID 118992,4-DichloronitrobenzeneHCID 109999031-(4-Aminobutyl)-4-(2-methoxyphenyl)piperazine

Product 1

HCID 23369409HCID 23369409, compound

Procedure

The compound was prepared according to the method described in Farmaco Ed. Sci. 36, 359 (1981) from 2,4-dichloronitrobenzene and 4-(2-methoxyphenyl)-1-piperazinbutanamine. M.p. 227°-229° C. as hydrochloride salt.

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-7c46917b88fd41f9a382dcaf3373b4e8
Source dataset
uspto-grants-1996_11
Patent number
US05576318

Reaction notes

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