HRID1900576

反应详情

EQUATION

反应方程式

HRID 1900576 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

1.1 mmol of 3-[[(1,1-dimethylethoxy)carbonyl](2-thienylmethyl)amino]-propanoic acid (16), prepared as described above in Example 16, was reacted with 8-chlorodibenz[b,f][1,4]-oxazepine-10(11H)-carboxylic acid, hydrazide (1), prepared as described above in Example 1, in the same manner described in Example 9. The yield of product was 0.31 g (51%). Analysis calculated for C27H29N4O5SCl 0.25 H2O (M.W. 561.57): C, 57.29.; H, 5.34; N, 9.90. Found: C, 57.42; H, 5.40; N, 9.96.

WORKUP

后处理

  1. customprepared