HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 23369659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 23369674 | HCID 23369674 | — |
| Product | HCID 23369659 | HCID 23369659 | 90.1% |
Reaction Steps
Reaction, past-process, and recrystallization (chloroform-methanol-ether) were performed in a manner similar to that described in Example 277 using 6-(2-methyl-2-propenyl)-5-hydroxy-3,8-dimethylcarbostyril (3.29 g, 13.54 mmol) and N-bromsuccinimide (2.41 g, 13.54 mmol). As a result, 3.93 g of the title compound was obtained as pale yellow prisms (90.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-221835fc20674cb58f0fcb5735c7d996 |
| Source note | uspto-grants-1996_11 |