HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 23369714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 23369768 | HCID 23369768 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 23369714 | HCID 23369714 | 72.7% |
Reaction Steps
A mixture of the compound obtained in Example 289 (3.30 g, 9.9 mmol), sodium azide (3.84 g, 59 mmol) and dimethylformamide (30 ml) was allowed to react at 120° C. for 4 hours. The reaction mixture was poured into water to obtain 2.13 g of the title compound as a pale brown solid (72.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-7e896b56b8184a42941d5a521083a7ef |
| Source note | uspto-grants-1996_11 |