HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 23369804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 137226531 | HCID 137226531 | — |
| Product | HCID 23369804 | HCID 23369804 | 181.5% |
Reaction Steps
Using 6-allyl-5-hydroxy-3,3,8-trimethylcarbostyril (1.36 g, 3.28 mmol) and N-bromosuccinimide (1.12 g, 6.28 mmol), the procedure of Example 277 was followed (reaction, post-treatment, and recrystallization from chloroform-ether-n-hexane). 1.93 g of the title compound was obtained as colorless needles (94.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-0df358f958774215b9bed86999706140 |
| Source note | uspto-grants-1996_11 |