HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 23369619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 23369558 | HCID 23369558 | — |
| Solvent | Chloroform hexane | HCID 21585165 | — |
| Product | HCID 23369619 | HCID 23369619 | 74.2% |
Reaction Steps
Using 5-hydroxy-6-(2-methyl-2-propenyl)-3,3,8-trimethyl-3,4-dihydrocarbostyril (1.35 g, 5.18 mmol) and N-bromosuccinimide (968 mg, 5.44 mmol), the procedure of Example 299 was followed (reaction, post-treatment, and recrystallization from chloroform-hexane) to obtain 1.30 g of the title compound as colorless needles (74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-1fc35362dbe948f685243c10b270c0f9 |
| Source note | uspto-grants-1996_11 |