HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Azide → HCID 23369657, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 23369619 | HCID 23369619 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 23369657 | HCID 23369657 | 81.1% |
Reaction Steps
Using 2-bromomethyl-2,5,8,8-tetramethyl-2,3,6,7,8,9-hexahydrofuro[2,3-f]quinoline-7-one (1.28 g, 3.78 mmol) and sodium azide (1.96 g, 30.1 mmol), the procedure of Example 300 was followed (reaction, post-treatment, and recrystallization from ethyl acetate-hexane) to obtain 921 mg of the title compound as colorless needles (81%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-36c85e1cd132404d9e339186273614aa |
| Source note | uspto-grants-1996_11 |