HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 23369560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 23369663 | HCID 23369663 | — |
| Solvent | Chloroform hexane | HCID 21585165 | — |
| Product | HCID 23369560 | HCID 23369560 | 99.2% |
Reaction Steps
Using 3-ethyl-6-(2-methyl-2-propenyl)-5-hydroxy-8-methylcarbostyril (710 mg, 2.76 mmol) and N-bromosuccinimide (516 mg, 2.90 mmol), the procedure of Example 227 was followed (reaction, post-treatment, and recrystallization from chloroform-n-hexane) to obtain 920 mg of the title compound as pale yellow crystals (99.2%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576324 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-968de05691784b96ba2216f683c1d145 |
| Source note | uspto-grants-1996_11 |