HCID 903193, compound → HCID 16769101, compound

Participants

Reaction Steps

To a suspension of N-(4-dimethylaminophenyl)-2-nitrobenzamide (3.0 g) in ethanol (30 ml) was added a catalytic amount of 10% palladium/carbon and catalytic reduction was carried out at a pressure of 1-2.5 arms at room temperature for 4 hrs. After the filtration of 10 catalyst, the solvent was distilled off and crystallization of the residue from chloroform/ethyl acetate afforded N-(4-dimethylaminophenyl)-2-aminobenzamide (2.2 g, 79%).

Provenance & Evidence