HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21832139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromoacetone | HCID 11715 | — |
| Reactant | Methyl (2-hydroxyphenyl)acetate | HCID 89719 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 21832139 | HCID 21832139 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 3, but using 15.6 g of methyl 2-hydroxyphenylacetate, 34 g of bromoacetone, 25 g of potassium carbonate and 170 ml of dimethylformamide, the title compound was obtained having an Rf=0.39 (thin layer chromatography over silica gel, using a 3:1 by volume mixture of hexane and ethyl acetate as the developing solvent).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05576340 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-b48af994cf45451daf83b104774a60f2 |
| Source note | uspto-grants-1996_11 |