HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Butylthio)benzoic acid → 2-Butylsulphanyl-5-thiophenecarboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Butylthio)benzoic acid | HCID 421757 | — |
| Reactant | 2-Bromo-5-butylsulphanylthiophene | HCID 23367382 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | 2-Butylsulphanyl-5-thiophenecarboxylic acid | HCID 4739239 | — |
Reaction Steps
The experimental procedure is as described for compound 2, with use of compound 7 (8.99 g, 0.036 mol) and n-butyllithium (15.0 ml, 2.5M in hexane. 0.037 mol). A white solid was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578242 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-8312f6130b0a407f94984926913223b6 |
| Source note | uspto-grants-1996_11 |