4-(Butylthio)benzoic acid → 4-Pentylbenzoic acid

HRID 1901400Notes

Reaction equation

HRID 1901400 reaction equation
C(S[C:6]1[CH:14]=[CH:13][C:9]([C:10]([OH:12])=[O:11])=[CH:8][CH:7]=1)CCC.[Li]>>[CH2:8]([C:6]1[CH:7]=[CH:8][C:9]([C:10]([OH:12])=[O:11])=[CH:13][CH:14]=1)[CH2:7][CH2:6][CH2:14][CH3:13]

Participants

3

Reactant 2

HCID 4217574-(Butylthio)benzoic acidHCID 3028194Lithium

Product 1

HCID 334794-Pentylbenzoic acid

Procedure

The experimental procedure was as described for the preparation of e.g. compound 2 (i.e. pour the lithium salt onto cardice and acidify). A white solid was obtained.

Workup

  1. customA white solid was obtained

Sources & evidence

ORD record
ord-96c282f89c9a4ada8ffe78c56936bfc4
Source dataset
uspto-grants-1996_11
Patent number
US05578242

Reaction notes

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