HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Propylene glycol methyl ether acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Catalyst | Cobalt octoate | HCID 8696 | — |
| Solvent | Water | HCID 962 | — |
| Product | Propylene glycol methyl ether acetate | HCID 7946 | — |
| Product | Diacetone Alcohol | HCID 31256 | — |
Reaction Steps
Cobalt 2-ethylhexanoate was diluted with a solvent in a weight ratio of ethanol:acetylacetone=100:10 to a solid content of 5 wt % as calculated as oxide (solution J) Solution A1, solution C1, solution H and solution J were mixed in a weight ratio of solution A1 :solution C1 :solution H:solution J=40:15:30:15, and heat treatment was conducted at 40° C. for 20 minutes. Then, the solution was diluted with a solvent in a mixed solvent in a weight ratio of water:ethanol:propylene glycol monomethyl ether acetate:IPA:diacetone alcohol=5.3:22.5:38:23:10 to a solid content of 1.2 wt % to obtain a coating solution for a colored antistatic film.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05578377 |
| Source dataset | uspto-grants-1996_11 |
| ORD ID | ord-94582c60c3d945619348f52e44d7a42d |
| Source note | uspto-grants-1996_11 |