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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1901663Generated: October 30, 2026

Trifluoroacetic acid → HCID 15383928, compound

https://huagongshe.com/reaction/1901663

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 15383948HCID 15383948—
SolventDichloromethaneHCID 6344—
ProductHCID 15383928HCID 1538392880.9%

Reaction Steps

A procedure similar to that described in Example 1 was repeated, except that 0.96 g of 5-[4-{2(R)-[5(S)-(3-chlorophenoxymethyl)-2-oxooxazolidin-3-yl]propoxy}benzyl]-3-triphenylmethylthiazolidine-2,4-dione (prepared as described in Preparation 29), 4 ml of methylene chloride and 4 ml of trifluoroacetic acid were used, to give 0.52 g of the title compound having a melting point of 48° C. to 53° C. (softening) and having [α]D =+54.0° (methanol, c=1.000).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05578620
Source datasetuspto-grants-1996_11
ORD IDord-a629f28b86c646af8afac6d22255909c
Source noteuspto-grants-1996_11