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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1901664Generated: October 31, 2026

Trifluoroacetic acid → HCID 15383929, compound

https://huagongshe.com/reaction/1901664

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 15383949HCID 15383949—
SolventDichloromethaneHCID 6344—
ProductHCID 15383929HCID 1538392979.8%

Reaction Steps

A procedure similar to that described in Example 1 was repeated, except that 0.73 g of 5-[4-{2(S)-[5(R)-(3-chlorophenoxymethyl)-2-oxooxazolidin-3-yl]propoxy}benzyl]-3-triphenylmethylthiazolidine-2,4-dione (prepared as described in Preparation 37), 4 ml of methylene chloride and 4 ml of trifluoroacetic acid were used, to give 0.39 g of the title compound having a melting point of 55° C. to 60° C. (softening) and having [α]D =-52.4° (methanol, c=0.990).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05578620
Source datasetuspto-grants-1996_11
ORD IDord-6d2364fe8fa448ce822a0612ce2f628e
Source noteuspto-grants-1996_11