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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1901665Generated: October 31, 2026

Trifluoroacetic acid → HCID 15383930, compound

https://huagongshe.com/reaction/1901665

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 15383950HCID 15383950—
SolventDichloromethaneHCID 6344—
ProductHCID 15383930HCID 1538393078.3%

Reaction Steps

A procedure similar to that described in Example 1 was repeated, except that 286 mg of 5-[4-{2(S)-[5(S)-(3-chlorophenoxymethyl)-2-oxooxazolidin-3-yl]propoxy}benzyl]-3-triphenylmethylthiazolidine -2,4-dione (prepared as described in Preparation 41), 1 ml of trifluoroacetic acid and 1 ml of methylene chloride were used, to give 150 mg of the title compound, melting at 54° C. to 56° C. and having [α]D =+41.8° (methanol, c=0.975).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05578620
Source datasetuspto-grants-1996_11
ORD IDord-c08ba2c0f31b4827a8d85910b15e45f5
Source noteuspto-grants-1996_11