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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1901666Generated: October 31, 2026

Trifluoroacetic acid → HCID 15383931, compound

https://huagongshe.com/reaction/1901666

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 15383951HCID 15383951—
SolventDichloromethaneHCID 6344—
ProductHCID 15383931HCID 1538393173.4%

Reaction Steps

A procedure similar to that described in Example 1 was repeated, except that 0.57 g of 5-[4-{2(R)-[5(R)-(3-chlorophenoxymethyl)-2-oxooxazolidin-3-yl]propoxy}benzyl]-3-triphenylmethylthiazolidine-2,4-dione (prepared as described in Preparation 45), 2 ml of trifluoroacetic acid and 2 ml of methylene chloride were used, to give 280 mg of the title compound, melting at 52° C. to 53° C. and having [α]D =-39.7° (methanol, c=0.965).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05578620
Source datasetuspto-grants-1996_11
ORD IDord-1060a4b69cd54f0787c6ade4654439c7
Source noteuspto-grants-1996_11