Hydrazine → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Carbazate

HRID 1902138Notes

Reaction equation

HRID 1902138 reaction equation
Cl[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3].[NH2:17][NH2:18]>CO>[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)(=[O:3])[NH:17][NH2:18]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 540353651-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Cloroformate

Product 1

HCID 536527591-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Carbazate

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound is prepared by reacting the compound of Example 27 (1 mole) with hydrazine (1.1 mole), employing methanol as the solvent.

Sources & evidence

ORD record
ord-763bc18c75244f2a82aa52d5e9a26908
Source dataset
uspto-grants-1996_11
Patent number
US05578731

Reaction notes

Loading…