Methylhydrazine → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

HRID 1902139Notes

Reaction equation

HRID 1902139 reaction equation

Cl[C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3].[CH3:17][NH:18][NH2:19]>CO>[CH3:17][NH:18][NH:19][C:2]([O:4][CH:5]1[CH2:10][C:9]([CH3:12])([CH3:11])[N:8]([O:13][CH3:14])[C:7]([CH3:16])([CH3:15])[CH2:6]1)=[O:3]

Participants

4

Reactant 2

HCID 6061Methylhydrazine

HCID 540353651-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Cloroformate

Product 1

HCID 544690901-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Methylhydrazinecarboxylate

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound is prepared by reacting the compound of Example 27 (1 mole) with methylhydrazine (1.1 mole) in methanol.

Sources & evidence

ORD record: ord-b50d9ee2a7eb4b859e89f04fdbfd22bb
Source dataset: uspto-grants-1996_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05578731

Reaction notes

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