Methyl carbazate → 1-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Hydrazinocarbonylhydrazinecarboxylate

HRID 1902141Notes

Reaction equation

HRID 1902141 reaction equation
[C:1]([O:5][CH:6]1[CH2:11][C:10]([CH3:13])([CH3:12])[N:9]([O:14][CH3:15])[C:8]([CH3:17])([CH3:16])[CH2:7]1)(=[O:4])[NH:2][NH2:3].[C:18](OC)(=[O:21])[NH:19][NH2:20]>CO>[NH:19]([C:18]([NH:3][NH:2][C:1]([O:5][CH:6]1[CH2:7][C:8]([CH3:17])([CH3:16])[N:9]([O:14][CH3:15])[C:10]([CH3:12])([CH3:13])[CH2:11]1)=[O:4])=[O:21])[NH2:20]

Participants

4

Reactant 2

HCID 80519Methyl carbazateHCID 536527591-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl Carbazate

Product 1

HCID 542840721-Methoxy-2,2,6,6-tetramethylpiperidin-4-yl 2-Hydrazinocarbonylhydrazinecarboxylate

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The title compound is prepared by reacting the compound of Example 28 (1 mole) with methyl carbazate (1 mole) by refluxing the reaction mixture in methanol.

Sources & evidence

ORD record
ord-6a81b3c8785341339b9eb3eca665aab3
Source dataset
uspto-grants-1996_11
Patent number
US05578731

Reaction notes

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