HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid → NSC16738
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid | HCID 6101 | — |
| Reactant | 1-Decanol | HCID 8174 | — |
| Reactant | Vanillic Acid | HCID 8468 | — |
| Product | NSC16738 | HCID 226358 | 50% |
Reaction Steps
The n-decyl vanillate was synthesized by refluxing decyl alcohol with vanillic acid in the presence of p-toluenesulfonic acid. After removal of the unreacted alcohol, purification and recrystallization from n-pentane, the n-decyl vanillate had a melting point of 40°-40.5° C. (Yield: about 50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362510 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-b65ac591ef3141d3adf2f014520a93f7 |
| Source note | uspto-grants-1982_12 |