HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15575166, compound → HCID 15575176, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15575166 | HCID 15575166 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 15575176 | HCID 15575176 | — |
Reaction Steps
7-Methylspiro[benzo[b]thiophene-2(3H),1'-cyclopropan]-3-one was prepared by a similar procedure to that of Example 8 except for the use of 7-methyl-4',5'-dihydrospiro[benzo[b]thiophene-2(3H),3'(2'H)-furan]-3,2'-dione obtained in Reference Example 11. Pale yellow needles [from C2H5OH--H2O (1:1)], mp 74°-75° C. Anal. Calcd. for C11H10OS: C, 69.44; H, 5.30. Found: C, 69.32; H, 5.07.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362740 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-f2425512e5b34a63b8f9ece7d8dc3cee |
| Source note | uspto-grants-1982_12 |