HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15575170, compound → HCID 15575181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15575170 | HCID 15575170 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15575181 | HCID 15575181 | — |
Reaction Steps
5-Piperidinosulfonylspiro[benzo[b]thiophene-2(3H),1'-cyclopropan]-3-one was prepared by a similar procedure to that of Example 8 except for the use of 5-piperidinosulfonyl 4',5'-dihydrospiro[benzo[b]thiophene-2(3H),3'(2'H)-furan]-3,2'-dione obtained in Reference Example 17. Colorless prisms (from C2H5OH), mp 155.5°-157° C. Anal. Calcd. for C15H17NO3S: C, 55.70; H, 5.30; N, 4.33. Found: C, 55.74; H, 5.34; N, 4.50.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362740 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-ea1197e0caed43f48eb942a3807ee9ee |
| Source note | uspto-grants-1982_12 |