HuagongsheHuagongshe Chemistry Print Report · For research reference only
2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- → 2,4-Diamino-6-(5-aminopentyl)-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2H-Azepine, 3,4,5,6-tetrahydro-7-methoxy- | HCID 75657 | — |
| Reactant | Carbamimidamidomethanimidamide | HCID 176517607 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2,4-Diamino-6-(5-aminopentyl)-1,3,5-triazine | HCID 21298790 | — |
Reaction Steps
A mixture of biguanide (1.05 g.), 4,5,6,7-tetrahydro-2-methoxy-3H-azepine (1.27 g.) and ethanol (50 ml.) was heated under reflux for 18 hours, cooled and the solid that crystallised was collected to give 2,4-diamino-6-(5-aminopentyl)-1,3,5-triazine which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362728 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-57a998d2524b4a9290094e1b81e6afc1 |
| Source note | uspto-grants-1982_12 |