Sodium Hydroxide → HCID 70547446, compound

HRID 1902374Notes

Reaction equation

HRID 1902374 reaction equation
[CH3:1][C:2]([CH3:15])=[CH:3][C:4]1[CH:9]=[CH:8][C:7]([CH:10]([CH3:14])[C:11]([OH:13])=[O:12])=[CH:6][CH:5]=1.[OH-].[Na+:17]>>[CH3:1][C:2]([CH3:15])=[CH:3][C:4]1[CH:9]=[CH:8][C:7]([CH:10]([CH3:14])[C:11]([O-:13])=[O:12])=[CH:6][CH:5]=1.[Na+:17]

Participants

3

Reactant 2

HCID 14798Sodium HydroxideHCID 1563562-[4-(2-Methylpropenyl)phenyl]propionic Acid

Product 1

HCID 70547446HCID 70547446, compound

Procedure

Stoichiometric amounts of 2-(4-dimethylvinylphenyl)propionic acid and 1 N aqueous sodium hydroxide were stirred at room temperature for 30 minutes. The mixture was washed with 2×50 ml portions of ether and the aqueous solution evaporated to dryness to give the title compound as a white solid, m.p. 166°-168°. I.R. C=O stretch 1550-1560 cm-1.

Workup

  1. washThe mixture was washed with 2×50 ml portions of ether
  2. customthe aqueous solution evaporated to dryness

Sources & evidence

ORD record
ord-7999705095a24634afdbbc66b737ac2e
Source dataset
uspto-grants-1982_12
Patent number
US04362891

Reaction notes

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