HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 54460727, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | 1,3-Bis(phenylsulfanyl)propan-2-yl prop-2-enoate | HCID 23070534 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54460727 | HCID 54460727 | — |
Reaction Steps
A solution of 15 grams of 1,3-bis-(phenylthio)-2-propyl acrylate, 9.2 grams of dodecanethiol, and 1 milliliter of "Triton B" in 75 milliliters of ethanol was heated under reflux for 53/4 hours. The reaction mixture was allowed to cool and was then poured into water. The oil which precipitated was separated by extraction with toluene and the toluene solution was stripped on a rotary evaporator. There remained 24.0 grams of a light colored oil which was identified as 1,3-bis-(phenylthio)-2-propyl 3-(dodecylthio)propionate by means of its NMR spectrum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04362887 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-b69c2cad4eb04134a09a43c9ca61d26e |
| Source note | uspto-grants-1982_12 |