Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Lauryl Methacrylate | HCID 8906 | — |
| Solvent | 2-Methyldecane | HCID 23415 | — |
| Product | HCID 20565525 | HCID 20565525 | — |
Reaction Steps
40 g of methacrylic acid and 0.5 g of hydroquinone are added to 1 liter of Isopar G and maintained at about 90° C. for about 10 hours. Next, 40 grams of lauryl methacrylate, 18 g methyl methacrylate, and 0.5 g benzoyl peroxide are added to the reaction flask to initiate polymerization. Polymerization is continued for five hours to produce a methacrylic acid-lauryl methacrylate-methyl methacrylate terpolymer. The terpolymer solution/dispersion is added to about 100 grams of soluble precursor A and ball milled to produce a substantially homogeneous gel on the borderline of solubility in Isopar G.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04363863 |
|---|
| Source dataset | uspto-grants-1982_12 |
|---|
| ORD ID | ord-084cd59c3c8e4541ae7cdb1fc330c98f |
|---|
| Source note | uspto-grants-1982_12 |
|---|
