HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo(d)thiazol-2-amine → HCID 12874026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo(d)thiazol-2-amine | HCID 8706 | — |
| Reactant | p-Chlorophenacyl bromide | HCID 68303 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 12874026 | HCID 12874026 | — |
Reaction Steps
To a stirred solution of 7.5 parts of 2-aminobenzothiazole in 80 parts of acetonitrile are added 11.75 parts of 2-bromo-1-(4-chlorophenyl)ethanone and the whole is stirred for about 20 hours at room temperature. The precipitated product is filtered off, washed with acetonitrile, and dried, yielding 11.4 parts of 1-(4-chlorophenyl)-2-(2-imino-3(2H)-benzothiazolyl)ethanone hydrobromide; mp. 261°-272° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04364942 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-788eee8ea6904832bd681fe20efe7699 |
| Source note | uspto-grants-1982_12 |