HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → (2-t-Pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Ethyl 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylate | HCID 19978748 | — |
| Solvent | Water | HCID 962 | — |
| Product | (2-t-Pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylic acid | HCID 19978737 | 68.6% |
Reaction Steps
Ethyl 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylate (2.8 g.) and a solution of sodium hydroxide (0.54 g.) in water (20 ml.) were treated according to a similar manner to that of Preparation (6-5) to give brown powder of 2-(2-t-pentyloxycarbonylamino-1,3-thiazol-4-yl)glyoxylic acid (1.75 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04364943 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-9432e3877c9a42058233b249abb08d1e |
| Source note | uspto-grants-1982_12 |