Dichloromethane → HCID 20513699, compound

Participants

Reaction Steps

2-Thiocyanomethylthio-4,4-diethyl-5-methylenethiazoline, 23. gm, is added to 75 ml of dichloromethane. 0.72 gm of chlorine in 20 ml of dichloromethane is then added to the system. The system is stirred at room temperature for 1 hour. The system is then washed with saturated sodium bicarbonate solution, filtered and the organic solution dried over magnesium sulfate. The dichloromethane is removed by stripping to give the 2-thiocyanomethylthio-4,4-diethyl-5-dichloromethylenethiazoline.

Provenance & Evidence