HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 20217690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 178432341 | HCID 178432341 | — |
| Product | HCID 20217690 | HCID 20217690 | 70% |
Reaction Steps
4-[(4-CHLOROPHENYL)METHYL]-6,7-DIHYDRO-2,6,6-TRIMETHYL-3H-IMIDAZO[1,2-a]PURIN-9(4H)-ONE. The nitroso compound of Procedure 103 was catalytically hydrogenated to the diamino compound and then treated with acetic anhydride according to the method of Procedure 63. There resulted from this process the mono N-acetyl derivative of 8-[(4-chlorophenyl)methyl]-6,7-diaminoimidazo[1,2-a]pyrimidin-5-one, m.p. 155°-159° after recrystallization from isopropanol and drying under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04366156 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-5c4e8e6008c8418db7fd7fe2845e21ba |
| Source note | uspto-grants-1982_12 |