HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → 2,6-Dichloro-3-methoxyphenylisothiocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | 2,6-Dichloro-3-methoxyaniline | HCID 20513888 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,6-Dichloro-3-methoxyphenylisothiocyanate | HCID 20513849 | — |
Reaction Steps
60.7 g of 2,6-dichloro-3-methoxy-aniline are dissolved in 65 ml of toluene and treated with 25 ml of thiophosgene in 50 ml of toluene. The solution obtained is heated to boiling under reflux overnight and subsequently evaporated in vacuo. There is obtained 2,6-dichloro-3-methoxyphenylisothiocyanate of boiling point 99° (0.13 Torr).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04366160 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-3a1c97d5615a48b19d26889ac3cf7360 |
| Source note | uspto-grants-1982_12 |