HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → 4-(2',4',6'-Trifluorophenyl)-carbethoxysemicarbazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 2,4,6-Trifluoroaniline | HCID 67765 | — |
| Reactant | Ethyl 3-(chloroformyl)carbazate | HCID 84905 | — |
| Solvent | Toluene ethylacetate | HCID 21584019 | — |
| Product | 4-(2',4',6'-Trifluorophenyl)-carbethoxysemicarbazide | HCID 12904377 | — |
Reaction Steps
A toluene solution of 2,4,6-trifluoroaniline is reacted with 2-carbethoxyhydrazinecarbonyl chloride as described above in Example 1b, mp 177°-178° (ethyl acetate/toluene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04366320 |
| Source dataset | uspto-grants-1982_12 |
| ORD ID | ord-3574e8679a7842c585f3b7dcf2e120cf |
| Source note | uspto-grants-1982_12 |